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The flow rate is a main processing parameters effects morphology of electrosprayed particles. Increasing flow rate from 0.5 mL/h to 2 mL/h caused bigger electrosprayed particles size, but the aggregation happened when the flow rate increased to 4 mL/h. Furthermore, the desirable microspheres were formed using a suitable set of parameters: flow rate...
7 trang | Chia sẻ: honghp95 | Ngày: 02/12/2020 | Lượt xem: 955 | Lượt tải: 0
The results in this study indicated that, by the way of changing the morphology in the sample by using TEA to make the porous structure or altering the sulfur and carbon black contents to change the amount of cross-linking in the compound (the strong chemical bonds of the sulfur linkages between the chains of the rubber molecules and the strong int...
7 trang | Chia sẻ: honghp95 | Ngày: 02/12/2020 | Lượt xem: 992 | Lượt tải: 0
In this study, the silica from RHA was successfully synthesized by precipitation method at pH 7. The effect of experimental factors on the purity and the extracted yield of silica were studied and suitable synthesized conditions were determined as 1 N of NaOH, 120 minutes of reaction time, 5 N of HCl and 50 % volume of ethanol in the washing sol...
9 trang | Chia sẻ: honghp95 | Ngày: 02/12/2020 | Lượt xem: 1139 | Lượt tải: 1
In situ forming hydrogel composites consisted of tyramine conjugated gelatin, 4–hydroxyphenylacetic acid conjugated chitosan and BCP were successfully prepared via horseradish peroxidase mediated reaction in the presence of hydrogen peroxide. With a rapid gelation time at the physiological condition and controllable biodegradation rate, the hydr...
8 trang | Chia sẻ: honghp95 | Ngày: 02/12/2020 | Lượt xem: 761 | Lượt tải: 0
In conclusion, vertically well–aligned ZnO NW arrays have been successfully synthesized on graphene/Si substrate without catalyst or additives by a simple thermal evaporation method. The as–synthesized ZnO NWs had diameters in the range of 300–350 nm, lengths over several tens micrometers. The SEM, HRTEM, XRD and Raman measurements revealed that...
11 trang | Chia sẻ: honghp95 | Ngày: 02/12/2020 | Lượt xem: 953 | Lượt tải: 0
Research about the molecular–weight dependance on blends polymer X–CT images, we have demonstrated visually the dependance of PMMA molecular–weight (3 types of Mw) in blends PMMA/PA12/PP 1/1/1 using 3D X–CT microstructure analyzing system; and how about the phase structure of a ternary blends with 3D images. Learn how about the preparation of s...
5 trang | Chia sẻ: honghp95 | Ngày: 02/12/2020 | Lượt xem: 1021 | Lượt tải: 0
In this paper we described the successfull synthesis and characterization of a monofunctional benzoxazine monomer from cardanol, a by-product of cashew industry by a solventless method. The monomer structure were confirmed by the FTIR and 'H NMR spectroscopy. DSC results indicates that the long alkyl chain substituent at the meta position in C-Bz a...
9 trang | Chia sẻ: honghp95 | Ngày: 02/12/2020 | Lượt xem: 771 | Lượt tải: 0
By utilization of a four-step procedure, 4-azidomethyl)benzyl thiol was successfully prepared and the conditions of step II (mesylation of alcohol to methylsulfonate) were optimized. This compound bearing both the azide and thiol functionalities was further used to couple with an allyl-functionalized PU foam via the thiol-ene “click” reaction, wher...
8 trang | Chia sẻ: honghp95 | Ngày: 02/12/2020 | Lượt xem: 798 | Lượt tải: 0
Rice straw treated with the two–stage process composed of separating hemicellulose with acid sulfuric and lignin by the aid of sulfomethylation agent for 7 h may be used as raw material for hydrolysis reaction of cellulose into glucose in support of the catalyst. Successful synthesized carbon catalyst containing –SO3H functional groups via hydro...
7 trang | Chia sẻ: honghp95 | Ngày: 02/12/2020 | Lượt xem: 808 | Lượt tải: 0
Liquid TDI microcapsules were successfully synthesized by interfacial polymerization of PU prepolymer in oil–in–water emulsion. Spherical microcapsules with average diameter in the range 90 – 240 µm were manufactured by adjusting agitation rate over the range 1200–800 rpm. The core in microcapsules was about 40.5 wt% at agitation rate 1000 rpm, ...
7 trang | Chia sẻ: honghp95 | Ngày: 02/12/2020 | Lượt xem: 820 | Lượt tải: 0